Fixing of Negative intensities in scan data points error in X’pert Highscore - 26

In this video, I have shown the Rietveld refinement of XRD spectra using X’pert Highscore software. When performing Rietveld refinement through X’pert Highscore software we sometimes face many types of errors including the “Negative intensities in scan data points” error. In this video, I have shown how to overcome this error when performing Rietveld refinement. If you have any questions, ask them in the comment section below. For more videos, please subscribe to NanoWorld. Thank you. #NanoWorld ______________________________________ For more updates follow us on, Facebook:   / fascinatingnanoworld   Twitter:   / nanoworld8   Instagram:   / nanoworld85   Contact: [email protected] ______________________________________ Interpretation of SAED pattern | estimation of d-spacing & (khl) values    • Interpretation of SAED pattern | estimatio...   How to put a scale bar on SEM & TEM images (SEM/TEM data analysis)    • How to put a scale bar on SEM & TEM images...   No valid atomic position available (Rietveld refinement through X’pert Highscore)    • Fixing of valid atomic position available ...   Negative intensities in scan data points (Rietveld refinement through X’pert Highscore)    • Fixing of Negative intensities in scan dat...   Indexing XRD peaks with Miller indices (hkl) values using X’pert Highscore software    • Indexing XRD peaks with hkl values using X...   How to plot JCPDS card with the XRD data using OriginLab software    • How to plot JCPDS card with the XRD data u...   XRD data analysis using X’pert Highscore software    • XRD data analysis using X'pert highscore s...   Deconvolution of photoluminescence PL spectra (PL peaks fitting)    • Deconvolution of photoluminescence PL spec...   How to find peak position and FWHM of XRD data    • How to find peak position and FWHM of XRD ...   How to calculate crystallites (grain) size from XRD data?    • Crystallites (grain) size from XRD data us...   Estimation of grain size through modifies Scherrer equation    • Grain (crystallites) size through modified...   Crystallites size and strain using W-H plot method    • crystallites (grain) size and strain throu...   Calculation of nanoparticle size through SEM image    • nanoparticles size from SEM images - 02   How to find Miller indices of XRD peaks?    • How to label XRD peaks with Miller indices...   How to calculate d-spacing from XRD data?    • How to calculate d-spacing / interplaner s...   How to calculate lattice constant (a, b, c) values from the XRD data?    • How to calculate lattice constant (a,b,c) ...   How to calculate microstrain and dislocation density from XRD data?    • strain and dislocation density from XRD da...   How to calculate crystallinity from XRD data?    • how to calculate crystallinity from XRD da...   How to smooth XRD data?    • How to smooth data (XRD) using OriginLab s...   Baseline correction for XRD data    • Baseline correction for XRD, FTIR, and Ram...   Cyclic Voltammetry Data Analysis    • CV Data Analysis through OriginLab - Calcu...   How to find bandgap energy using the Tauc plot method?    • Video   How to calculate bandgap energy using the Kubelka Munk function?    • Video   Understanding Tauc plot, 1240 (constant) and 2.303 constant    • Video   How to know a material either have direct or indirect bandgap energy?    • Video   DSC Data Analysis    • DSC Analysis Through OriginLab - Enthalpy ...   TGA Data Analysis    • TGA Analysis Through OriginLab (Thermal pr...   How to plot the double Y-axis in a single graph?    • TGA & DSC double plot (double Y-axis in a ...   Electron paramagnetic resonance (EPR) data analysis (calculation of g-factor)    • Electron paramagnetic resonance data analy...   _________________________________________ Music Source Unconditionally by Broken Elegance 🎩   / brokenelegance   Creative Commons — Attribution 3.0 Unported — CC BY 3.0 http://creativecommons.org/licenses/b... Music promoted by Audio Library    • Unconditionally – Broken Elegance (No Copy...  

Fixing of valid atomic position available error in X’pert Highscore - 27
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Fixing of valid atomic position available error in X’pert Highscore - 27

XRD data analysis using X'pert highscore software - 23
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XRD data analysis using X'pert highscore software - 23

Tutorial de análise de difração de raio X (DRX) utilizando o X'Pert HighScore Plus
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Tutorial de análise de difração de raio X (DRX) utilizando o X'Pert HighScore Plus

How to subtract instrumental broadening (βi) from XRD data using origin
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How to subtract instrumental broadening (βi) from XRD data using origin

XRD Analysis search and match and  Phase Determination using X'Pert HighScore
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XRD Analysis search and match and Phase Determination using X'Pert HighScore

Crystallite Size & Microstrain - Part 1 - Scherrer Equation - HighScore Plus - Panalytical
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Crystallite Size & Microstrain - Part 1 - Scherrer Equation - HighScore Plus - Panalytical

XRD Analysis for Phase Determination using X'Pert HighScore Plus
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XRD Analysis for Phase Determination using X'Pert HighScore Plus

Indexing XRD peaks with hkl values using X'pert highscore - 25
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Indexing XRD peaks with hkl values using X'pert highscore - 25

X'pert HighScore:How to Index XRD Peaks With Miller Indices (hkl)(اندیس گذاری پیکهای پراش اشعه ایکس)
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X'pert HighScore:How to Index XRD Peaks With Miller Indices (hkl)(اندیس گذاری پیکهای پراش اشعه ایکس)

Building the Raman System: Lasers and FT-Raman
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Building the Raman System: Lasers and FT-Raman

HighScore Plus Tutorial - Phase Quantification Rietveld X-ray Diffraction - Long Version - JIAM
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HighScore Plus Tutorial - Phase Quantification Rietveld X-ray Diffraction - Long Version - JIAM

Introduction to Dynamic Light Scattering Analysis
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Introduction to Dynamic Light Scattering Analysis

Introduction to X-ray Diffraction
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Introduction to X-ray Diffraction

Solution to the Problem - No Valid Atoms in Highscore Plus - What to Do if You Can't Refine a Phase
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Solution to the Problem - No Valid Atoms in Highscore Plus - What to Do if You Can't Refine a Phase

Introduction to Rietveld Analysis by Prof  Ashish Garg, IIT Kanpur
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Introduction to Rietveld Analysis by Prof Ashish Garg, IIT Kanpur

Part-1 Rietveld Refinement using X-pert High Score
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Part-1 Rietveld Refinement using X-pert High Score

An introduction to gas sorption analysis, pore size and BET surface area measurement
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An introduction to gas sorption analysis, pore size and BET surface area measurement

How to do Reitveld Refinement using X'pert Highscore Plus | Electroceramics Lab
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How to do Reitveld Refinement using X'pert Highscore Plus | Electroceramics Lab

HighScore Plus Tutorial - Phase Identification X-ray Diffraction - Long Version - JIAM Diffraction
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HighScore Plus Tutorial - Phase Identification X-ray Diffraction - Long Version - JIAM Diffraction

Phase identification from XRD data with Profex
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Phase identification from XRD data with Profex